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Yoshida, Kenta*; Toyama, Takeshi*; Inoue, Koji*; Nagai, Yasuyoshi*; Shimodaira, Masaki
Materia, 62(3), p.154 - 158, 2023/03
no abstracts in English
Takamizawa, Hisashi; Hata, Kuniki; Nishiyama, Yutaka; Toyama, Takeshi*; Nagai, Yasuyoshi*
Journal of Nuclear Materials, 556, p.153203_1 - 153203_10, 2021/12
Times Cited Count：3 Percentile：44.61(Materials Science, Multidisciplinary)Solute clusters (SCs) formed in pressurized water reactor surveillance test specimens neutron-irradiated to a fluence of 1 
10
n/cm
were analyzed via atom probe tomography to understand the effect of silicon on solute clustering and irradiation embrittlement of reactor pressure vessel steels. In high-Cu bearing materials, Cu atoms were aggregated at the center of cluster surrounded by the Ni, Mn, and Si atoms like a core-shell structure. In low-Cu bearing materials, Ni, Mn, and Si atoms formed cluster and these solutes were not comprised core-shell structure in SCs. While the number of Cu atoms in clusters was decreased with decreasing nominal Cu content, the number of Si atoms had clearly increased. The cluster radius (
) and number density (
) decreased and increased, respectively, with increasing nominal Si content. The shift in the reference temperature for nil-ductility transition (
RT
) showed a good correlation with the square root of volume fraction (
) multiplied by r (
). This suggested that the dislocation cutting through the particles mechanism dominates the precipitation hardening responsible for irradiation embrittlement. The negative relation between the nominal Si content and RT indicated that increasing of nominal Si content reduces the degree of embrittlement.
Takamizawa, Hisashi; Shimizu, Yasuo*; Inoue, Koji*; Nozawa, Yasuko*; Toyama, Takeshi*; Yano, Fumiko*; Inoue, Masao*; Nishida, Akio*; Nagai, Yasuyoshi*
Applied Physics Express, 9(10), p.106601_1 - 106601_4, 2016/10
Times Cited Count：0 Percentile：0(Physics, Applied)Ueno, Fumiyoshi; Komatsu, Atsushi; Igarashi, Takahiro; Yamamoto, Masahiro
Proceedings of European Corrosion Congress 2014 (EUROCORR 2014) (USB Flash Drive), 10 Pages, 2014/09
In this paper, the effect of phosphorous concentration in grain boundary (GB) on intergranular corrosion (IC) progress was studied to understand GB corrosion behavior of stainless steels in boiling nitric acid solution. Phosphorus (P) added extra high purity type 310 stainless alloy was corroded in boiling nitric acid solution, and P in GB was detected by three-dimensional atom probe. IC progress considering with P profile in GB was studied by numerical simulation using cellular automaton method. As the results, we concluded that P concentration change around 1.4at% in GB of the alloy caused IC rate change in boiling nitric acid solution. The developed numerical method could simulate GB corrosion change with P distribution in GB.
Kikuchi, Kenji*; Okada, Noriyuki*; Kato, Mikio*; Uchida, Hiroshi*; Saito, Shigeru
Journal of Nuclear Materials, 450(1-3), p.237 - 243, 2014/07
Times Cited Count：3 Percentile：23.79(Materials Science, Multidisciplinary)Three-dimensional atom probe techniques were applied to the investigation on the oxide scale in 12Cr ferritic-martensitic steel, HCM12A. A duplex oxide scale was formed in lead bismuth eutectic at 450-500
C, during 5500 h. Samples were located 500-700 nm away from the boundary between magnetite and Fe-Cr spinel layers, while the total oxide layer thickness is 18 
m. It detected super enrichment of Cr with a size of ten nm roughly, as well as depletion of Fe and enrichment of O at the same site. Surrounding the Cr super enrichment area, enrichment of Si was newly noticed due to the scanned profile of detected atom counts. It is also confirmed that Pb and Bi concentration in the observed spinel region is almost null or less than 0.01 atomic percent, which is possible detecting lowest limit.
Du, Y.*; Toyama, Takeshi*; Inoue, Koji*; Otsuka, Satoshi; Yano, Yasuhide; Yoshida, Kenta*; Shimada, Yusuke*; Onuma, Masato*; Mitsuhara, Masatoshi*; Nakashima, Hideharu*; et al.
no journal, ,
